WELCOME TO CHEMISTRY 2001-section Summer 2018  Section 1

Office: Chemistry Department,  room 201A  Choppin Hall

INSTRUCTOR- Professor  : Dr. Kresimir Rupnik, Ph. D. 

   E-mail: rupnik@intelliom.com    or chrupn@lsu.edu          Phone/cell                  205-1353

  Lecture and Lab Rooms       201 Williams lectures  and Williams 302 lab demonstrations

       1:20-2:20PM: M- F. Because of the character of the lab demonstrations and reviews additional small group activities will be scheduled out of that time according to students convenience (see form in the syllabus)

 Office hours: please email or phone for appointment.  Flexible time is much better for students than fixed office hours. You are most welcome to stop by when I am in office or call if I am in a  lab !

 

You can contact me any time if you have questions. 

 SYLLABUS-

NOTE: you must have a notebook (pages with numbers) for this class in order to better study and communicate with me and other students. It must contain insight into all your class activities and work in and out of the class. Bring it when you talk with me.

SCANNED TABLES (handouts)

MATERIAL-TEXTBOOK

 

 

NEWS:  We will have dates of exams a week after classes start

Final exam is …………….., check LSU website, in our classroom .

Final (LSU schedule):

 Bring the tables-handouts and calculators

 YOUR INPUT e-mail if you have comments                                                                                                                                 

CHAPTERS/

SCHEDULE

ASSIGNED MATERIAL

 

NEWS

Chapters; 0, 1, 2

 

 

Start reading this first::

Part 1 /Chapter 0-1   introduction, units, sample preparation etc.

Notes on ppm

Tools of the trade $ Excel (Chapter 2)

.

We will work on acid base equilibrium later, however you need to start practice and test your stoichiometry skills now. There will be a review dedicated to this material.

in

 

Exam1
tentatively June 20

 

 

PRACTICE

 

Chapter 3 lecture notes (uncertainty/error direct and propagated)

Chapter 4 &5 lecture notes/ supplement (how to use mathematics /statistics to simplify uncertainty and represent data with confidence)

 

IN CLASS ASSIGNMENT

1 2 3 4 5 6 7

RBC      time measurement

 

TABLES YOU will  NEED -handouts in the class --
Table 4-2 Student's t value

Table 3-1 Propagation of uncertainty

FYI: *Propagation of uncertainty-derivation (only for your information, lecture supplement) 

 Pdf Excel-example: temperature conversion

 

PART 4 SHORT

 Part 4 - calibration and uncertainty, comments on sensitivity

ultrasensitivity etc

NEW: EXCEL TABLE 4-7

Excel- example calibration function and linear regression

EXCEL-calibration Fig 5-9

EXCEL problem 5-2

 

 

 

 

 

 

 

Chapters

17-21...

\

exam 2 tentative July 6… or after

 

 


..



Part 3 -1 spectroscopy
Spectroscopy little helper figures

Part 3-2 instruments

Part 3-3 atomic absorption

(Additional assignment:

LABWORK:- lab visit

FLUORESCENCE 2014http://www.nobelprize.org/nobel_prizes/chemistry/laureates/2014/

pH measurements               quz

FTIR                                      quiz

AAS                                   quiz

FLUORESCENCE                      quiz)

 

 quiz -5 spectroscopy

 hw4   (answers)

hw5 (answer)

hw 6 ( answers )

quiz -6 spectroscopy

PREXAM2

answ

STUDY MATERIAL 2

 

PREEXAM quizzes

 

 

 

Introduction to equilibrium (see CHEM 1201/1202)

Acid and Base single component solution equilibrium

CHARGE and MASS balance

Buffer - acid conjugate base mixture equilibrium

Titration in analytical chemistry

Example Excel - finding volume from titeration 7 (derivatives)

Polyprotic titration

ADDITIONAL MATERIAL:

Excel-titration base

Strong acids textbook p 108.

Excel data from a titration of diprotic acid - precise identification of end points in a pH-volume diagram

EDA (ethylene diamine) diprotic titration

HOW to make a buffer (example)

Buffer example-blood 1

pH second example 2

Electrochemistry of pH electrodes p 306 (chapter15-5)

Smallest titration p 216, Fluorescence- titration p 158

Complete mass and charge balances FYI

1 ca and mg ions

2-titr

figure excess titration

 

MS

 

Activity

.

quiz 1 2  in class
HW7=practice set 2

  guide to answers=same answers ps2

preEXAM aqueous equilibrium

  answers (in class)

 

 

 

 

 

 

 

Chapters 22-24...

 

 

practice exams 1-3

 

 

Chromatography - Separations Chemistry

part 6-1

part 6-2

List of problems : Resolution and Plate hights, HPLC instrument, GC instrument, HPLC chromatogram and GC chromatogram

hw 7

hw7 answers

quiz

 

 

ELECTROCHEMISTRY